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Kinetic aspects of the nanocrystallization and evolution of microhardness in Al92-xNi8Lax amorphous alloys
K.L. Sahoo, R. Sahu,
Published in
2007
Volume: 22
   
Issue: 4
Pages: 497 - 501
Abstract
Marginal glass forming Al-based alloys have attracted considerable attention due to the occurrence of a primary crystallization reaction that yields a microstructure consisting of uniformly dispersed Al-nanocrystals embedded in an amorphous matrix. Rapidly solidified Al-alloys ribbons containing 8 at.% Ni and 4-6 at.% La were prepared by single roller melt-spinning technique. As-melt-spun and annealed ribbons were investigated by means of differential scanning calorimetry (DSC), X-ray diffractometry (XRD) and hardness measurements. XRD studies revealed that ribbons are fully amorphous in the as-melt-spun state. DSC studies showed that crystallization proceeds in two or three stages that are sensitively influenced by La content. Crystallizations kinetics were analysed by Kissinger and Johnson-Mehl-Avrami approaches. Microhardness of all the ribbons was examined at different temperatures and correlated with the corresponding structural evolution.
About the journal
JournalMaterials and Manufacturing Processes
ISSN10426914